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Beilstein J. Org. Chem. 2022, 18, 1249–1255, doi:10.3762/bjoc.18.130
Graphical Abstract
Scheme 1: Methods for the synthesis of thiazoles using active methylene ketones as starting materials.
Scheme 2: Substrate scope. Reaction conditions: 1 (2 mmol), 2 (1 mmol), NH4I (0.1 mmol), ᴅʟ-alanine (1 mmol),...
Scheme 3: Up-scaling experiment.
Scheme 4: Control experiments.
Scheme 5: The proposed mechanism for the one-pot electrochemical synthesis of 2-aminothiazoles mediated by NH4...